文章摘要
瞿发林,谈丽娜,赵勇,刘桂永.HPLC法测定舒筋活络酒中阿魏酸的含量[J].药学与临床研究,2007,15(4):321~323
HPLC法测定舒筋活络酒中阿魏酸的含量
Determination of ferulic acid in Shujin Huoluo Jiu by HPLC
投稿时间:2007-01-15  
DOI:
中文关键词: 高效液相色谱法  舒筋活络酒  阿魏酸
英文关键词: HPLC  Shujin Huoluo Jiu (SHJ)  Ferulic acid
基金项目:
作者单位
瞿发林 解放军第102医院药械科 
谈丽娜 解放军第102医院药械科 
赵勇 解放军第102医院药械科 
刘桂永 解放军第102医院药械科 
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中文摘要:
      目的:建立舒筋活络酒中阿魏酸的含量测定方法。方法:采用高效液相色谱法测定舒筋活络酒中阿魏酸的含量。色谱柱为YMC-Pack(ODS-A,φ5 μm,150 mm×4.6 mm);流动相为甲醇-1%乙酸(20∶80);流速 1.0 mL·min-1;检测波长为 320 nm。结果:阿魏酸的线性范围为0.038~1.216 μg,r=0.9997;回收率为97.41%,RSD为1.64%。结论:本法操作简
英文摘要:
      Objective:To establish a HPLC method for the determination of ferulic acid in Shujin Huoluo Jiu. Methods: Separation and quantitation were carried on the YMC-Pack ODS-A column(5 μm, 150 mm×4.6 mm) with mobile phase consists of methanol-1% acetic acid (20∶80). The detection wavelength was 320 nm. The flow rate was 1.0 mL·min-1. Results: The assay was linear over the range of 0.038~1.216 μg. The average recovery was 97.41%, RSD was 1.64% (n=6). Conclusions: The assay is simple, sensitive and accurate, which can be applied in quality control of Shujin Huoluo Jiu.
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